Julien Guinet's recipes

How to Make Indelible Black Ink

Natural ink made by Julien Guinet

The history of this indelible ink

This ink was already known to the Egyptians as early as 2,500 BC. In Europe, it was not until the Middle Ages that iron gall ink became widespread and the preferred writing medium for eight centuries. It is valued because it is simple to make and remarkably stable: ancient manuscripts written with this ink have retained all the intensity of their black. In France, it remained the only ink in use until around 1850. Artists used it particularly for line work and washes, alongside bistre, sepia, and later India ink, which is much more viscous. Indelible and highly fluid, it became standard for official documents, to the point of being nicknamed “civil registry ink” in the 19th century.

This is not India ink. It is an iron gall-tannate ink, also known as iron gall ink or metallo-gallic ink. It is made from ferrous sulfate and plant-based tannins, whereas India ink is produced from “lampblack,” a pigment created by the incomplete combustion of resinous wood or other carbon-rich organic materials.

The Recipe

Minimum 10 days

Easy

Average cost

Ingredients

Utensils

Bottle
1 bottle (1 L)

Preferably tinted

Mixing bowl
1 container

Bowl type

Whisk
1 whisk
Measuring spoon
1 measuring spoon
Funnel
1 funnel
Sieve
1 fine-mesh strainer
Saucepan
1 saucepan
Cloth Filter
1 cloth coffee filter

Or a fine cloth

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Important

  • I strongly recommend following the recipe exactly, because the iron in this ink can become very corrosive on paper after a few years if the proportions are not correct!
  • This recipe produces a truly INDELIBLE black ink that stains heavily, so I recommend wearing gloves and an apron.
  • To avoid any danger, it is important not to use the equipment used in this recipe for cooking.

Preparation

Step 1
  • Place the gall nuts in the mortar and crush them until you get a fine powder.

If the gall nuts are too hard, wrap them in an old cloth you no longer use and hit them with a hammer to break them up roughly before putting them in the mortar. You can also use an electric coffee grinder.

How to Make Ink
Make ink
Step 2
  • Bring about 700 ml of distilled water to a boil in the saucepan, then add the gall nut powder. Lower the heat and cook over very low heat (≃ 65 °C) for about two hours.

Ensure the water does not evaporate completely and add more if necessary.

make indelible black ink
make indelible black ink
make indelible black ink
Step 3
  • Let cool for a few minutes, then pour the mixture into the container, filtering it through the cloth coffee filter (or fine cloth).
How to Make Black Ink
Step 4
  • In one of the jars, mix the ferrous sulfate with 200 ml of distilled water using a wooden stick or a spoon (that you will no longer use for eating).

Avoid mixing with an iron object.

Ink recipe – step 4
Step 5
  • Pour this mixture into the container holding the gall nut juice, then add 3 drops of clove essential oil.

When it comes into contact with ferrous sulfate, the gall nut juice will darken.

Ink recipe – step 5
Step 6

If you already have ready-made liquid gum arabic, skip this step.

However, if you have chosen gum arabic in grain (crystal) or powder form, you must prepare your gum water.

  • Pour 5 g of gum arabic and 10 ml of distilled water into a jar. You can then wait 24 hours for the gum to dissolve, or heat it in a double boiler to speed up the process.
  • Using the fine-mesh strainer, filter the gum arabic water directly into the second jar to remove impurities.

You now have gum water.

Ink recipe – step 6
make indelible black ink
Ink recipe – step 7
Step 7
  • Measure 10 ml of gum water and pour it into the container containing the gall nut juice.
  • Mix with the whisk.
Indelible ink
Step 8
  • Pour the contents of the bowl into the bottle using the funnel.
Recipe for making Indelible Black Ink
Step 9
  • Your ink is almost ready! Let it rest for 10 days in a cool, dry place without sealing the bottle.

This time allows the iron to oxidize properly when exposed to air, which makes the ink blacker.

How to Make Your Own Ink

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